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Allergy (rare): swelling, hives, wheezing stop use and seek medical help

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The flow was set to 1 mL/min, with an injection volume of 10 L, using a gradient of acetonitrile (A) and ultrapure water + trifluoroacetic acid 0.05% (B): 0 min, 0:100 (A:B)

The acid's backflow irritates the food pipe lining & may cause inflammation