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Preliminarily, fresh and used filters were subjected to characterization by LCSM technique for determining fibres morphology, and by ICP/MS and COD analyses for evaluating amounts of contaminants (see supplemental information)

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In the former case, the increment of concentration of aqueous H 3 PO 4 up to 2.0 M resulted in a neglectable increase of yield in levulinic acid respect to preliminary experiments, thus suggesting that 1.5 M is the best value (Table 1, entries 5, 1112)