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The analytes were resolved on an Acquity UPLC high strength silica (HSS) perfluorophenyl (PFP) (150 mm 2.1 mm, 1.8 m) column (Waters Inc., MA) maintained at 40C, using a binary gradient consisting of 0.2% formic acid (Solvent A) and methanol (Solvent B)

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The Chaini Khaini 3-D capture revealed nicely cut material, however the Zarda items were coarsely cut and sized irregularly (Fig

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