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Before NMR analysis, the sample was reconstituted in 50 l of precooled 4 C methanol, centrifuged at 18,500 g for 10 minutes at 4 C and the resulting supernatant was transferred into a precooled 2 ml Eppendorf and then stored at -80 C [25]

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[DOI] [PubMed] [Google Scholar] 105.Ayoub B.M., Mowaka S., Safar M.M., Ashoush N., Arafa M., Michel H., Tadros M.M., Elmazar M.M., Mousa S