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The 200 mg cigar sample was weighed and placed in a 1.5 mL centrifugation tube, and 10 L internal standard (10 ppm L-2-chlorophenylalanine) and 1000 L extract solution (methanol/acetonitrile/water, 2:2:1) were added, vortexed for 1 min, and subjected to ultrasound for 30 min